Technology Process of C26H26BrF4N3O5
There total 12 articles about C26H26BrF4N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 24h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium azide / water; acetone / 3 h / Heating / reflux
2: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C
3: dichloromethane / 20 °C
4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
5: boron tribromide / dichloromethane / -70 - 20 °C
6: triethylamine / dichloromethane / 24 h / 20 °C
With
sodium azide; di-isopropyl azodicarboxylate; hydrogen; boron tribromide; triethylamine; triphenylphosphine;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetone;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydroxide; water; tetra-(n-butyl)ammonium iodide / dichloromethane / 168 h / 20 °C
2: sodium azide / water; acetone / 3 h / Heating / reflux
3: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C
4: dichloromethane / 20 °C
5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
6: boron tribromide / dichloromethane / -70 - 20 °C
7: triethylamine / dichloromethane / 24 h / 20 °C
With
sodium hydroxide; sodium azide; di-isopropyl azodicarboxylate; water; hydrogen; boron tribromide; tetra-(n-butyl)ammonium iodide; triethylamine; triphenylphosphine;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetone;