2--3,4,6-trifluorobenzoic acid

Base Information

Chemical Name:2--3,4,6-trifluorobenzoic acid
CAS No.:123016-62-6
Molecular Formula:C₁₆H₁₂F₃NO₃
Molecular Weight:323.271
Hs Code.:

2-<acetyl(phenylmethyl)amino>-3,4,6-trifluorobenzoic acid

Synonyms:2--3,4,6-trifluorobenzoic acid

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Chemical Property of 2--3,4,6-trifluorobenzoic acid

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Technology Process of 2--3,4,6-trifluorobenzoic acid

There total 4 articles about 2--3,4,6-trifluorobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108-24-7
acetic anhydride

: 123016-61-5
3,4,6-trifluoro-2-<(phenylmethyl)amino>benzoic acid

: 123016-62-6
2--3,4,6-trifluorobenzoic acid

Guidance literature:: With dmap; triethylamine;
DOI:10.1021/jm00107a039

Reference yield:

: 32890-92-9
2,3,4,6-tetrafluorobenzoic acid

: 123016-62-6
2--3,4,6-trifluorobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / conc. H₂SO₄ / 68 h / Heating

2: 70 percent / Et₃N / acetonitrile / 2 h / Heating

3: 93 percent / 2N NaOH / methanol / 72 h / Heating

4: 82 percent / Et₃N, 4-(dimethylamino)pyridine

With dmap; sodium hydroxide; sulfuric acid; triethylamine; In methanol; acetonitrile;
DOI:10.1021/jm00107a039

Reference yield:

: 53001-68-6
methyl 2,3,4,6-tetrafluorobenzoate

: 123016-62-6
2--3,4,6-trifluorobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / Et₃N / acetonitrile / 2 h / Heating

2: 93 percent / 2N NaOH / methanol / 72 h / Heating

3: 82 percent / Et₃N, 4-(dimethylamino)pyridine

With dmap; sodium hydroxide; triethylamine; In methanol; acetonitrile;
DOI:10.1021/jm00107a039