N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester

Base Information

Chemical Name:N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester
CAS No.:133166-95-7
Molecular Formula:C₁₇H₁₅BrClFN₂O₃
Molecular Weight:429.673
Hs Code.:

Synonyms:N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester

Chemical Property:

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Technology Process of N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester

There total 3 articles about N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 133166-93-5
6-chloro-2-<(4-bromo-2-fluorophenyl)methyl>-2H-3,1-benzoxazine-2,4(1H)-dione

: 133166-95-7
N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester

Guidance literature:: With triethylamine; In toluene; at 100 ℃; for 4h;
DOI:10.1021/jm00108a038

Reference yield:

: 4743-17-3
5-Chloroisatoic anhydride

: 133166-95-7
N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH (80percent dispersion in mineral oil) / 1.) DMF, 2 h, 2.) 8 h

2: Et₃N / toluene / 4 h / 100 °C

With sodium hydride; triethylamine; In toluene;
DOI:10.1021/jm00108a038

Reference yield:

: 76283-09-5
4-bromo-2-fluorobenzyl bromide

: 133166-95-7
N-<2-<<(4-bromo-2-fluorophenyl)methyl>amino>-6-chlorobenzoyl>glycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH (80percent dispersion in mineral oil) / 1.) DMF, 2 h, 2.) 8 h

2: Et₃N / toluene / 4 h / 100 °C

With sodium hydride; triethylamine; In toluene;
DOI:10.1021/jm00108a038