(η6-3-(trimethylsilyl)indene)tricarbonylchromium

Base Information

• Chemical Name: (η6-3-(trimethylsilyl)indene)tricarbonylchromium
• CAS No.: 261353-67-7
• Molecular Formula: C₁₅H₁₆CrO₃Si
• Molecular Weight: 324.372
• Mol file: 261353-67-7.mol

Synonyms:(η6-3-(trimethylsilyl)indene)tricarbonylchromium

Chemical Property of (η6-3-(trimethylsilyl)indene)tricarbonylchromium

Chemical Property:

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Technology Process of (η6-3-(trimethylsilyl)indene)tricarbonylchromium

There total 1 articles about (η6-3-(trimethylsilyl)indene)tricarbonylchromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3-Trimethylsilylinden (18053-75-3) + chromium(0) hexacarbonyl (199620-14-9,13007-92-6) → (η6-3-(trimethylsilyl)indene)tricarbonylchromium (261353-67-7)

Guidance literature:

In tetrahydrofuran; under N2 atm. to soln. 1-(trimethylsilyl)indene in n-butyl ether was added THF and Co(CO)6, mixt. was heated at reflux for 72 h; solvents were removed under vac., residue was subjected flash chromy. on silica using hexane as eluent; elem. anal.;

DOI:10.1021/om990650f

upstream raw materials:

3-Trimethylsilylinden

chromium⁽⁰⁾ hexacarbonyl