1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide

Base Information

• Chemical Name: 1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide
• CAS No.: 1415219-11-2
• Molecular Formula: C₂F₆NO₄S₂*C₉H₂₀N
• Molecular Weight: 422.413
• Mol file: 1415219-11-2.mol

Synonyms:1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide

Chemical Property of 1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide

There total 2 articles about 1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methylpyrrolidin (34375-89-8) + N-methyl-3-methylpyrrolidine (45470-22-2) + 4-amino-2-methyl-1-butanol (44565-27-7,44565-28-8,64070-19-5,88390-32-3) + propyl bromide (106-94-5) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → 1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide (1415219-11-2)

Guidance literature:

With sodium hydroxide; formaldehyd; formic acid; magnesium sulfate; triphenylphosphine; In tetrachloromethane; dichloromethane; water, 1,3-dimethyl-1-propylpyrrolidinium bromide; water;

Reference yield:

4-amino-2-methyl-1-butanol (44565-27-7,44565-28-8,64070-19-5,88390-32-3) → 1,3-dimethyl-1-propylpyrrolidinium bis(trifluoromethanesulfonyl)amide (1415219-11-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: triphenylphosphine; tetrachloromethane / dichloromethane / 40 °C / Inert atmosphere

1.2: 12 h

2.1: formic acid / 1.5 h / 100 °C / Cooling

3.1: dichloromethane / 24 h / Reflux

4.1: water

With tetrachloromethane; formic acid; triphenylphosphine; In dichloromethane; water;

upstream raw materials:

3-methylpyrrolidin

N-methyl-3-methylpyrrolidine

4-amino-2-methyl-1-butanol

propyl bromide