dibenzyl 3,8-dioxodecandioate

Base Information

Chemical Name:dibenzyl 3,8-dioxodecandioate
CAS No.:417707-99-4
Molecular Formula:C₂₄H₂₆O₆
Molecular Weight:410.467
Hs Code.:

Synonyms:dibenzyl 3,8-dioxodecandioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl 3,8-dioxodecandioate

Chemical Property:

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Technology Process of dibenzyl 3,8-dioxodecandioate

There total 1 articles about dibenzyl 3,8-dioxodecandioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 111-69-3
hexanedinitrile

: 5437-45-6
Benzyl bromoacetate

: 417707-99-4
dibenzyl 3,8-dioxodecandioate

Guidance literature:: hexanedinitrile; Benzyl bromoacetate; With copper; zinc; In tetrahydrofuran; for 2h; Heating;

With hydrogenchloride;
DOI:10.1055/s-2002-19305

Reference yield: 29.0%

: 123-54-6,81235-32-7
acetylacetone

: 417707-99-4
dibenzyl 3,8-dioxodecandioate

: 417708-00-0
1,4-bis(4-acetyl-2-benzyloxycarbonyl-5-methyl-3-pyrrolyl)butane

Guidance literature:: dibenzyl 3,8-dioxodecandioate; With acetic acid; sodium nitrite; In tetrahydrofuran; at 20 ℃; for 1h;

acetylacetone; With sodium acetate; acetic acid; zinc; In tetrahydrofuran; for 14h;
DOI:10.1055/s-2002-19305

Reference yield:

: 417707-99-4
dibenzyl 3,8-dioxodecandioate

: 417708-01-1
1,4-bis(2-benzyloxycarbonyl-4-ethyl-5-methyl-3-pyrrolyl)butane

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. NaNO₂; AcOH / tetrahydrofuran / 1 h / 20 °C

1.2: 29 percent / Zn; AcOH; NaOAc / tetrahydrofuran / 14 h

2.1: 92 percent / NaBH₄; BF₃*Et₂O / tetrahydrofuran / 1 h / 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; acetic acid; sodium nitrite; In tetrahydrofuran; 1.1: Knorr reaction;
DOI:10.1055/s-2002-19305