N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine

Base Information

• Chemical Name: N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine
• CAS No.: 84562-58-3
• Molecular Formula: C₁₅H₁₄BrCl₂N₃
• Molecular Weight: 387.106

Synonyms:N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine

Chemical Property of N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine

Chemical Property:

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Technology Process of N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine

There total 2 articles about N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3-bromo-4-(N,N-dimethylamino)benzaldehyde (56479-63-1) + 2,6-dichloro-p-phenylenediamine (609-20-1) → N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine (84562-58-3)

Guidance literature:

In ethanol; for 1.5h; Heating;

DOI:10.1021/jm00378a030

Reference yield:

4-nitro-2,6-dichloroaniline (99-30-9) → N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine (84562-58-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / SnCl₂, HCl aq.

2: 81 percent / ethanol / 1.5 h / Heating

With hydrogenchloride; tin(ll) chloride; In ethanol;

DOI:10.1021/jm00378a030

Reference yield: 62.0%

N'-[1-(3-Bromo-4-dimethylamino-phenyl)-meth-(E)-ylidene]-2,6-dichloro-benzene-1,4-diamine (84562-58-3) → N'-(3-Bromo-4-dimethylamino-benzyl)-2,6-dichloro-benzene-1,4-diamine (85103-77-1)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; for 18h; Ambient temperature;

DOI:10.1021/jm00378a030

upstream raw materials:

3-bromo-4-(N,N-dimethylamino)benzaldehyde

2,6-dichloro-p-phenylenediamine

4-nitro-2,6-dichloroaniline

Downstream raw materials:

N'-(3-Bromo-4-dimethylamino-benzyl)-2,6-dichloro-benzene-1,4-diamine

N'-[4-(3-Bromo-4-dimethylamino-benzylamino)-2,6-dichloro-phenyl]-N,N-dimethyl-formamidine

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