1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid

Base Information

Chemical Name:1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid
CAS No.:116467-30-2
Molecular Formula:C₂₀H₂₂ClNO₂*ClH
Molecular Weight:380.314
Hs Code.:

Synonyms:1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid

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Chemical Property of 1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid

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Technology Process of 1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid

There total 3 articles about 1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 116467-29-9
2-<2-(4,5-Dihydro-7,8-dimethoxy-3H-2-benzazepin-1-yl)phenyl>-ethanol-hydrochlorid

: 116467-30-2
1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid

Guidance literature:: With trichlorophosphate; at 60 ℃; for 0.25h;

Reference yield:

: 108010-37-3
N-<3-(3,4-Dimethoxyphenyl)propyl>-2-<2-(ethoxycarbonyloxy)ethyl>benzamid

: 116467-30-2
1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / POCl₃ / acetonitrile / 6 h / Heating

2: 91 percent / 20percent KOH / ethanol / 12 h / Ambient temperature

3: 79 percent / POCl₃ / 0.25 h / 60 °C

With potassium hydroxide; trichlorophosphate; In ethanol; acetonitrile;

Reference yield:

: 116467-28-8
Kohlensaeure-<2-<2-(4,5-dihydro-7,8-dimethoxy-3H-2-benzazepin-1-yl)phenyl>ethyl>ester-hydrochlorid

: 116467-30-2
1-<2-(2-Chlorethyl)phenyl>-7,8-dimethoxy-4,5-dihydro-3H-2-benzazepin-hydrochlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 20percent KOH / ethanol / 12 h / Ambient temperature

2: 79 percent / POCl₃ / 0.25 h / 60 °C

With potassium hydroxide; trichlorophosphate; In ethanol;