4--1-methyl-5-methylaminocarbonylimidazole

Base Information

• Chemical Name: 4--1-methyl-5-methylaminocarbonylimidazole
• CAS No.: 107605-86-7
• Molecular Formula: C₁₅H₁₇ClN₄O₂
• Molecular Weight: 320.779

Synonyms:4--1-methyl-5-methylaminocarbonylimidazole

Chemical Property of 4--1-methyl-5-methylaminocarbonylimidazole

Chemical Property:

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Technology Process of 4--1-methyl-5-methylaminocarbonylimidazole

There total 1 articles about 4--1-methyl-5-methylaminocarbonylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

caffeidine (20041-90-1) + α-chlorophenylacetyl chloride (2912-62-1) → 4--1-methyl-5-methylaminocarbonylimidazole (107605-86-7)

Guidance literature:

With triethylamine; In chloroform; for 1h; Ambient temperature;

DOI:10.1248/cpb.34.3573

Reference yield: 70.0%

4--1-methyl-5-methylaminocarbonylimidazole (107605-86-7) → 6-phenyl-1,4,7-trimethyl-5,8-dioxo-1,4,5,6,7,8-hexahydroimidazo<4,5-e><1,4>diazepine (107605-90-3)

Guidance literature:

With sodium hydride; In ethanol; at 60 - 70 ℃; for 1h;

DOI:10.1248/cpb.34.3573

Reference yield: 38.0%

4--1-methyl-5-methylaminocarbonylimidazole (107605-86-7) → 6-phenyl-1,4-dimethyl-5,8-dioxo-1,4,5,8-tetrahydro-6H-imidazo<4,5-e><1,4>oxazepine (107605-93-6)

Guidance literature:

In water; for 2h; Heating;

DOI:10.1248/cpb.34.3573

upstream raw materials:

caffeidine

α-chlorophenylacetyl chloride

Downstream raw materials:

6-phenyl-1,4-dimethyl-5,8-dioxo-1,4,5,8-tetrahydro-6H-imidazo<4,5-e><1,4>oxazepine

6-phenyl-1,4,7-trimethyl-5,8-dioxo-1,4,5,6,7,8-hexahydroimidazo<4,5-e><1,4>diazepine

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