(S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

Base Information

Chemical Name:(S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester
CAS No.:1007217-08-4
Molecular Formula:C₂₄H₃₆N₂O₃Si
Molecular Weight:428.647
Hs Code.:

Synonyms:(S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

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Chemical Property of (S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

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Technology Process of (S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

There total 1 articles about (S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₄N₄O₃Si

: 1007217-08-4
(S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

Guidance literature:: C₂₄H₃₄N₄O₃Si; With triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 12h;

With water; In tetrahydrofuran; at 20 ℃; for 12h; Further stages.;
DOI:10.1021/ja7102394

Reference yield: 94.0%

: 1007217-08-4
(S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

: 2459-05-4
(E)-4-ethoxy-4-oxobut-2-enoic acid

: 1373889-07-6
C₃₀H₄₂N₂O₆Si

Guidance literature:: With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja302711z

Reference yield: 81.0%

: 863647-70-5
trans-3-phenylbenzylcarbamoylpropenoic acid

: 1007217-08-4
(S)-3-amino-2-(tert-butyldiphenylsilanyloxy)propylcarbamic acid tert-butyl ester

: 1007217-10-8
C₄₁H₄₉N₃O₅Si

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12h;
DOI:10.1021/ja7102394