4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide

Base Information

Chemical Name:4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide
CAS No.:1601476-95-2
Molecular Formula:C₁₆H₁₂F₆N₂O₂S
Molecular Weight:410.34
Hs Code.:

Synonyms:4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide

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Technology Process of 4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide

There total 1 articles about 4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 74853-66-0
4'-trifluoromethyl-2,2,2-trifluoroacetophenone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1601476-95-2
4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide

Guidance literature:: In toluene; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201304143

Reference yield: 70.0%

: 1601476-95-2
4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide

: 536-74-3
phenylacetylene

: 1-(1,1-difluoro-4-phenylbut-1-en-3-yn-2-yl)-4-(trifluoromethyl)benzene

Guidance literature:: With copper(l) iodide; tetrabutyl-ammonium chloride; lithium trifluoromethanesulfonate; lithium tert-butoxide; In 1,4-dioxane; at 60 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.5b00980

Reference yield: 69.0%

: 1601476-95-2
4-methyl-N'-(2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethylidene)benzenesulfonohydrazide

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 7-(trifluoromethyl)-7-(4-(trifluoromethyl)phenyl)cyclohepta-1,3,5-triene

Guidance literature:: With caesium carbonate; In neat (no solvent); at 120 ℃; for 3h; Molecular sieve; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0034-1378937