bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate

Base Information

Chemical Name:bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate
CAS No.:389866-44-8
Molecular Formula:C₆₃H₆₆N₂O₁₀
Molecular Weight:1011.22
Hs Code.:

Synonyms:bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate

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Chemical Property of bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate

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Technology Process of bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate

There total 8 articles about bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1663-67-8
malonoyl dichloride

: 389866-43-7
4'-cyano-[1,1'-biphenyl]-4-yl 4-((10-hydroxydecyl)oxy)benzoate

: 389866-44-8
bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/b103798f

Reference yield:

: 53463-68-6
1-bromo-10-decanol

: 389866-44-8
bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / 4 M aq. NaOH / ethanol / 22 h / Heating

2: 81 percent / DMAP; DCC / CH₂Cl₂ / 20 h / 20 °C

3: 92 percent / Et₃N / CH₂Cl₂ / 18 h / 20 °C

With dmap; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1039/b103798f

Reference yield:

: 19812-93-2
4-Cyano-4'-hydroxybiphenyl

: 389866-44-8
bis(10-(4-(((4'-cyano-[1,1'-biphenyl]-4-yl)oxy)carbonyl)phenoxy)decyl) malonate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / DMAP; DCC / CH₂Cl₂ / 20 h / 20 °C

2: 92 percent / Et₃N / CH₂Cl₂ / 18 h / 20 °C

With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/b103798f