C₂₈H₃₃N₃O₂

Base Information

Chemical Name:C₂₈H₃₃N₃O₂
CAS No.:87923-86-2
Molecular Formula:C₂₈H₃₃N₃O₂
Molecular Weight:443.589
Hs Code.:

C<sub>28</sub>H<sub>33</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₈H₃₃N₃O₂

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Chemical Property of C₂₈H₃₃N₃O₂

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Technology Process of C₂₈H₃₃N₃O₂

There total 5 articles about C₂₈H₃₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 588-59-0
stilbene

: 87923-86-2
C₂₈H₃₃N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 97.6 percent / monoperphthalic acid / diethyl ether / 18 h / Ambient temperature

2: 16.2 g / 1.) n-BuLi / 1.) THF, -78 deg C, 0.75 h, 2.) -78 deg C, 4 h; RT, 6 h

3: 1.) n-BuLi, 2.) LiAlH₄ / 1.) dioxane-hexane, 0 deg C -> RT, 2.) reflux, 20 h

4: 95.3 percent / pyridinium hydrobromide perbromide / acetic acid; CCl₄ / 8 h / Ambient temperature

5: 1.) LiF, Li₂CO₃ / 1.) HMPA, 60 deg C, 22 h, 2.) EtOAc, reflux, 24 h

With lithium aluminium tetrahydride; n-butyllithium; monoperoxyphthalic acid; pyridinium hydrobromide perbromide; lithium carbonate; lithium fluoride; In tetrachloromethane; diethyl ether; acetic acid;
DOI:10.1021/ja00364a031

Reference yield:

: 87923-83-9
cis-1-phenyl-7,8-dimethylbicyclo<4.2.0>octa-3,7-diene

: 87923-86-2
C₂₈H₃₃N₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: 95.3 percent / pyridinium hydrobromide perbromide / acetic acid; CCl₄ / 8 h / Ambient temperature

2: 1.) LiF, Li₂CO₃ / 1.) HMPA, 60 deg C, 22 h, 2.) EtOAc, reflux, 24 h

With pyridinium hydrobromide perbromide; lithium carbonate; lithium fluoride; In tetrachloromethane; acetic acid;
DOI:10.1021/ja00364a031

Reference yield:

: 87923-82-8
cis-1-phenyl-8-thiabicyclo<4.3.0>non-3-ene 8,8-dioxide

: 87923-86-2
C₂₈H₃₃N₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: 16.2 g / 1.) n-BuLi / 1.) THF, -78 deg C, 0.75 h, 2.) -78 deg C, 4 h; RT, 6 h

2: 1.) n-BuLi, 2.) LiAlH₄ / 1.) dioxane-hexane, 0 deg C -> RT, 2.) reflux, 20 h

3: 95.3 percent / pyridinium hydrobromide perbromide / acetic acid; CCl₄ / 8 h / Ambient temperature

4: 1.) LiF, Li₂CO₃ / 1.) HMPA, 60 deg C, 22 h, 2.) EtOAc, reflux, 24 h

With lithium aluminium tetrahydride; n-butyllithium; pyridinium hydrobromide perbromide; lithium carbonate; lithium fluoride; In tetrachloromethane; acetic acid;
DOI:10.1021/ja00364a031