38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.1^32,36]octatriconta-32,34,Δ^36,38-triene

Base Information

• Chemical Name: 38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.1^32,36]octatriconta-32,34,Δ^36,38-triene
• CAS No.: 811431-74-0
• Molecular Formula: C₅₇H₇₈N₆O₁₃S₄
• Molecular Weight: 1183.54

Synonyms:38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.1^32,36]octatriconta-32,34,Δ^36,38-triene

Chemical Property of 38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.1^32,36]octatriconta-32,34,Δ^36,38-triene

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Technology Process of 38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.1^32,36]octatriconta-32,34,Δ^36,38-triene

There total 3 articles about 38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.1^32,36]octatriconta-32,34,Δ^36,38-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) + C45H58N6O9S4 (811431-71-7) → 38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.132,36]octatriconta-32,34,Δ36,38-triene (811431-74-0) + 2,6-bis[4,13-bis(4-toluensulfonyl)1,4,13-triaza-7,10-dioxacyclopentadec-1-ylmethyl]-1-methoxybenzene

Guidance literature:

With sodium ethanolate; In ethanol; N,N-dimethyl-formamide; at 110 ℃; for 8h;

DOI:10.1039/b408808e

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → 38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.132,36]octatriconta-32,34,Δ36,38-triene (811431-74-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / Et₃N / CHCl₃ / 24 h / 20 °C

2: 4.5 percent / NaOEt / ethanol; dimethylformamide / 8 h / 110 °C

With sodium ethanolate; triethylamine; In ethanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1039/b408808e

Reference yield:

2,6-bis{[bis(2-aminoethyl)amino]methyl}anisole → 38-methoxy-4,13,19,28-tetrakis(4-toluensulfonyl)-1,4,13,16,19,28-hexaaza-7,10,22,25-tetraoxatricyclo[14.14.7.132,36]octatriconta-32,34,Δ36,38-triene (811431-74-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / Et₃N / CHCl₃ / 24 h / 20 °C

2: 4.5 percent / NaOEt / ethanol; dimethylformamide / 8 h / 110 °C

With sodium ethanolate; triethylamine; In ethanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1039/b408808e

upstream raw materials:

triethylene glycol di-(p-toluenesulfonate)

C₄₅H₅₈N₆O₉S₄

p-toluenesulfonyl chloride

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