Technology Process of C19H24BrN3O4
There total 1 articles about C19H24BrN3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium acetate;
In
toluene;
at 100 ℃;
for 19h;
- Guidance literature:
-
C19H24BrN3O4;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
for 1h;
(2-trimethylethylsilylethoxy)methyl chloride;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
With
ammonium chloride;
In
water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C
1.2: 20 °C
2.1: diisobutylaluminium hydride / dichloromethane; hexane / 5 h / -78 °C
2.2: 0.25 h / 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C
3.2: 15 h / 20 °C
4.1: hydrogenchloride / 1,4-dioxane / 5 h / 50 °C
With
hydrogenchloride; sodium hydride; diisobutylaluminium hydride;
In
1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;