C₃₀H₄₀N₄O₉

Base Information

Chemical Name:C₃₀H₄₀N₄O₉
CAS No.:1391396-51-2
Molecular Formula:C₃₀H₄₀N₄O₉
Molecular Weight:600.669
Hs Code.:

C<sub>30</sub>H<sub>40</sub>N<sub>4</sub>O<sub>9</sub>

Synonyms:C₃₀H₄₀N₄O₉

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Chemical Property of C₃₀H₄₀N₄O₉

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Technology Process of C₃₀H₄₀N₄O₉

There total 13 articles about C₃₀H₄₀N₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 46460-82-6,55895-87-9,84907-81-3
O-benzyl-L-serine methyl ester

: C₁₉H₂₇N₃O₇

: 1391396-51-2
C₃₀H₄₀N₄O₉

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.75h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: C₁₆H₂₆N₂O₆

: 1391396-51-2
C₃₀H₄₀N₄O₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethanol

3.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

4.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

5.2: 12 h / -20 - 20 °C / Inert atmosphere

6.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

6.2: pH 1 / Acidic conditions

7.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1064764-00-6
methyl 2-(2-methyl-2-tert-butoxy-1-tert-butoxycarbonylamino-ethyl)-oxazole-4-carboxylate

: 1391396-51-2
C₃₀H₄₀N₄O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

1.2: pH 1 / Acidic conditions

2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / ethanol

4.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

6.2: 12 h / -20 - 20 °C / Inert atmosphere

7.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

7.2: pH 1 / Acidic conditions

8.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.05.105