phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside
CAS No.:1356031-22-5
Molecular Formula:C₄₉H₅₅N₇O₈SSi
Molecular Weight:930.169
Hs Code.:

phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

Synonyms:phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

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Chemical Property of phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

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Technology Process of phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

There total 9 articles about phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₁H₄₉N₇O₆SSi

: 501-53-1,94274-21-2
benzyl chloroformate

: 1356031-22-5
phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2011.11.088

Reference yield:

: phenyl 2-azido-3-O-benzyl-2-deoxy-1-thio-β-D-galactopyranoside

: 1356031-22-5
phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2 h

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Molecular sieve

3: sodium methylate; tert-butyl alcohol / 2 h / 20 °C

4: ethylenediamine / tert-butyl alcohol / 1 h / Reflux

5: sodium hydrogencarbonate / tetrahydrofuran; water

With 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydrogencarbonate; ethylenediamine; tert-butyl alcohol; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.11.088

Reference yield:

: 1372074-05-9
phenyl 4-O-(2-azido-3-O-benzoyl-4-phthalimido-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

: 1356031-22-5
phenyl 4-O-(2-azido-4-benzyloxycarbonylamino-2,4,6-trideoxy-α-D-galactopyranosyl)-2-azido-3-O-benzyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate; tert-butyl alcohol / 2 h / 20 °C

2: ethylenediamine / tert-butyl alcohol / 1 h / Reflux

3: sodium hydrogencarbonate / tetrahydrofuran; water

With sodium methylate; sodium hydrogencarbonate; ethylenediamine; tert-butyl alcohol; In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2011.11.088