isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate

Base Information

Chemical Name:isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate
CAS No.:1520080-39-0
Molecular Formula:C₁₆H₂₇NO₄Si
Molecular Weight:325.48
Hs Code.:

Synonyms:isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate

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Chemical Property of isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate

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Technology Process of isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate

There total 4 articles about isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₃₅NO₄Si₂

: 1520080-39-0
isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/ol403142d

Reference yield:

: 672-13-9
2-hydroxy-5-methoxybenzaldehyde

: 1520080-39-0
isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / 1 h / 20 °C

1.2: 0.5 h / 0 - 20 °C

2.1: tetrahydrofuran; acetone; water / 2 h / 0 - 20 °C

3.1: tetra-N-butylammonium tribromide / methanol; dichloromethane / 1 h / 0 - 20 °C

4.1: triethylamine / dichloromethane-d2 / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran / 2.5 h / -78 - 20 °C / Inert atmosphere

With n-butyllithium; tetra-N-butylammonium tribromide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; dichloromethane-d2; water; acetone;
DOI:10.1021/ol403142d

Reference yield:

: 1520080-37-8
isopropyl 2-hydroxy-5-methoxybenzyl(methyl)carbamate

: 1520080-39-0
isopropyl 2-hydroxy-5-methoxy-3-(trimethylsilyl)benzyl(methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-N-butylammonium tribromide / methanol; dichloromethane / 1 h / 0 - 20 °C

2: triethylamine / dichloromethane-d2 / 0 - 20 °C / Inert atmosphere

3: n-butyllithium / tetrahydrofuran / 2.5 h / -78 - 20 °C / Inert atmosphere

With n-butyllithium; tetra-N-butylammonium tribromide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; dichloromethane-d2;
DOI:10.1021/ol403142d