4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid

Base Information

• Chemical Name: 4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid
• CAS No.: 1187975-91-2
• Molecular Formula: C₃₁H₄₆N₂O₅Si
• Molecular Weight: 554.802

Synonyms:4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid

Chemical Property of 4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid

Chemical Property:

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Technology Process of 4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid

There total 1 articles about 4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C37H60N2O5Si2 → 4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid (1187975-91-2)

Guidance literature:

With water; potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

DOI:10.1016/j.bmcl.2009.06.065

Reference yield: 48.0%

3-amino-5-(methanesulfonyl(methyl)amino)-N-((R)-1-phenylethyl)benzamide (1187976-09-5) + 4-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-4-(tert-butyldimethylsilanyloxy)-6-phenylhexanoic acid (1187975-91-2) → 2-(tert-butyldimethylsilanyloxy)-2-phenethylpentanedioic acid 1-[((S)-1-benzylcarbamoyl-2-methylpropyl)amide] 5-{[3-(methanesulfonyl(methyl)amino)-5-((R)-1-phenylethylcarbamoyl)phenyl]amide}

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 50 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.06.065

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