anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Base Information

Chemical Name:anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide
CAS No.:80484-77-1
Molecular Formula:C₁₅H₁₁NO₃S₂
Molecular Weight:317.389
Hs Code.:

Synonyms:anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

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Chemical Property of anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

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Technology Process of anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

There total 4 articles about anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 80484-76-0
anhydro-2-<2-(phenylthio)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

: 80484-77-1
anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Guidance literature:: With peracetic acid; In dichloromethane; at -5 - 0 ℃; for 0.333333h;
DOI:10.1021/jo00345a050

Reference yield:

: 10002-29-6
S-(2-pyridyl)thioglycolic acid

: 80484-77-1
anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 0.5 h / Heating

2: 46 percent / NaH / dimethylformamide / 18 h / Ambient temperature

3: 48 percent / peracetic acid / CH₂Cl₂ / 0.33 h / -5 - 0 °C

With peracetic acid; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo00345a050

Reference yield:

: 80484-75-9
C₉H₆ClNO₂S

: 80484-77-1
anhydro-2-<2-(phenylsulfinyl)acetyl>-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / NaH / dimethylformamide / 18 h / Ambient temperature

2: 48 percent / peracetic acid / CH₂Cl₂ / 0.33 h / -5 - 0 °C

With peracetic acid; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00345a050