1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole

Base Information

Chemical Name:1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole
CAS No.:1383717-82-5
Molecular Formula:C₃₂H₃₁N₃O₃
Molecular Weight:505.616
Hs Code.:

Synonyms:1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole

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Chemical Property of 1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole

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Technology Process of 1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole

There total 9 articles about 1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1383717-81-4
1,5-bis-benzyloxy-2-isopropyl-4-azido-benzene

: 10602-04-7
(4-ethynylphenyl)methanol

: 1383717-82-5
1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole

Guidance literature:: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

Reference yield: 72.0%

: 10602-04-7
(4-ethynylphenyl)methanol

: C₂₃H₂₁N₃O₂

: 1383717-82-5
1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole

Guidance literature:: With chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm401536b

Reference yield:

: 1155371-80-4
(((4-isopropyl-1,3-phenylene)bis(oxy))bis(methylene))dibenzene

: 1383717-82-5
1-[2,4-bis(benzyloxy)cumenyl]-5-[p-(hydroxymethyl)phenyl]-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid; acetic acid / 0.67 h / 70 - 80 °C

2.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 4 h / 80 °C

2.2: 0 °C

3.1: trimethylsilylazide; tert.-butylnitrite / acetonitrile / 13 h / 0 - 20 °C

4.1: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With hydrogenchloride; tert.-butylnitrite; trimethylsilylazide; nitric acid; acetic acid; tin(ll) chloride; chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; In ethanol; water; N,N-dimethyl-formamide; acetonitrile;