all-trans-12-fluororetinal

Base Information

Chemical Name:all-trans-12-fluororetinal
CAS No.:108448-49-3
Molecular Formula:C₂₀H₂₇FO
Molecular Weight:302.432
Hs Code.:

Synonyms:all-trans-12-fluororetinal

Suppliers and Price of all-trans-12-fluororetinal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of all-trans-12-fluororetinal

Chemical Property:

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Technology Process of all-trans-12-fluororetinal

There total 4 articles about all-trans-12-fluororetinal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 857636-72-7
(11-Z)-12-fluororetinonitrile

: 108448-49-3
all-trans-12-fluororetinal

Guidance literature:: With diisobutylaluminium hydride; In hexane; Petroleum ether; at -80 - -40 ℃; for 1h;
DOI:10.1002/ejoc.200400488

Reference yield:

: 78843-78-4
3-methyl-4-oxo-2-butenenitrile

: 108448-49-3
all-trans-12-fluororetinal

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / 6 h / 131 °C

2: 31 percent / (diethylamino)sulfur trifluoride / CH₂Cl₂ / 20 °C

3: 40 mg / NaH / tetrahydrofuran / 0 - 20 °C

4: 98 percent / DIBAL-H / petroleum ether; hexane / 1 h / -80 - -40 °C

With diethylamino-sulfur trifluoride; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane; Petroleum ether;
DOI:10.1002/ejoc.200400488

Reference yield:

: 844881-08-9
4-(diphenoxyphosphoryl)-4-fluoro-3-methyl-2-butenenitrile

: 108448-49-3
all-trans-12-fluororetinal

Guidance literature:: Multi-step reaction with 2 steps

1: 40 mg / NaH / tetrahydrofuran / 0 - 20 °C

2: 98 percent / DIBAL-H / petroleum ether; hexane / 1 h / -80 - -40 °C

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; Petroleum ether;
DOI:10.1002/ejoc.200400488