1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole

Base Information

Chemical Name:1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole
CAS No.:1352750-96-9
Molecular Formula:C₃₉H₄₃N₃O₆
Molecular Weight:649.787
Hs Code.:

Synonyms:1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole

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Chemical Property of 1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole

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Technology Process of 1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole

There total 3 articles about 1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 80894-21-9
1-azido-2-methoxy-ethane

: 287962-77-0
(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-2-(benzyloxymethyl)-6-ethynyl-tetrahydropyran

: 1352750-96-9
1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole

Guidance literature:: With copper; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In dichloromethane; water; tert-butyl alcohol; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1ob06317k

Reference yield:

: 3866-62-4,3964-13-4,56822-48-1,56822-49-2,78136-22-8,80300-30-7,83462-68-4,83462-69-5,94943-10-9,80300-97-6
2,3,4,6-tetra-O-benzyl-D-galactopyranosyl acetate

: 1352750-96-9
1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / Inert atmosphere

2: sodium hydroxide / methanol; dichloromethane / Inert atmosphere

3: copper; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / dichloromethane; water; tert-butyl alcohol / 20 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; copper; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c1ob06317k

Reference yield:

: 443915-85-3
trimethyl-[2-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]ethynyl]silane

: 1352750-96-9
1-(2-methoxyethyl)-4-[(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-6-(benzyloxymethyl)tetrahydropyran-2-yl]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol; dichloromethane / Inert atmosphere

2: copper; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / dichloromethane; water; tert-butyl alcohol / 20 °C / Inert atmosphere

With copper; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c1ob06317k