C₆₉H₁₁₄N₁₀O₁₄

Base Information

• Chemical Name: C₆₉H₁₁₄N₁₀O₁₄
• CAS No.: 1306770-59-1
• Molecular Formula: C₆₉H₁₁₄N₁₀O₁₄
• Molecular Weight: 1307.72
• Mol file: 1306770-59-1.mol

Synonyms:C₆₉H₁₁₄N₁₀O₁₄

Chemical Property of C₆₉H₁₁₄N₁₀O₁₄

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₆₉H₁₁₄N₁₀O₁₄

There total 2 articles about C₆₉H₁₁₄N₁₀O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N,N'-(4,4'-methylene-bis(1,4-phenylene))bis(2-chloroacetamide) (17328-15-3) + 1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester hydrochloride (173526-92-6) → C69H114N10O14 (1306770-59-1)

Guidance literature:

With sodium carbonate; In acetonitrile; Inert atmosphere; Heating;

DOI:10.1021/ic2004672

Reference yield:

4,4'-diamino diphenyl methane (101-77-9) → C69H114N10O14 (1306770-59-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water / 4 h / 20 °C / Inert atmosphere

2: sodium carbonate / acetonitrile / Inert atmosphere; Heating

With sodium carbonate; sodium hydroxide; In water; acetonitrile;

DOI:10.1021/ic2004672

Reference yield: 90.0%

C69H114N10O14 (1306770-59-1) → [(CH2CH2NCH2COOH)3CH2CH2NCH2CONHC6H4]2CH2 (1306770-62-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/ic2004672

upstream raw materials:

N,N'-(4,4'-methylene-bis(1,4-phenylene))bis(2-chloroacetamide)

1,4,7,10-tetraazacyclododecane-1,4,7-triacetic acid tris(1,1-dimethylethyl) ester hydrochloride

4,4'-diamino diphenyl methane

Downstream raw materials:

[(CH₂CH₂NCH₂COOH)3CH₂CH₂NCH₂CONHC₆H₄]2CH₂

Refernces