C₅₂H₉₀O₁₂SSi₂

Base Information

Chemical Name:C₅₂H₉₀O₁₂SSi₂
CAS No.:1316279-00-1
Molecular Formula:C₅₂H₉₀O₁₂SSi₂
Molecular Weight:995.516
Hs Code.:

C<sub>52</sub>H<sub>90</sub>O<sub>12</sub>SSi<sub>2</sub>

Synonyms:C₅₂H₉₀O₁₂SSi₂

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Chemical Property of C₅₂H₉₀O₁₂SSi₂

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Technology Process of C₅₂H₉₀O₁₂SSi₂

There total 26 articles about C₅₂H₉₀O₁₂SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1316278-99-5
C₅₂H₈₉IO₁₂SSi₂

: 1316279-00-1
C₅₂H₉₀O₁₂SSi₂

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; water; at 0 - 20 ℃; for 3h;

Reference yield:

: 1139773-78-6
C₁₆H₂₅NO₅

: 1316279-00-1
C₅₂H₉₀O₁₂SSi₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 16 h / 0 - 23 °C

2.2: 0.5 h / 0 - 10 °C

3.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 22 °C

4.1: zinc / methanesulfonic acid / tetrahydrofuran / 5 h / Reflux

5.1: water; acetic acid / tetrahydrofuran / 10 h / 10 - 20 °C

6.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

7.1: toluene / 0.25 h / 95 °C

8.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 1 h / -30 - -25 °C

9.1: hydrogenchloride / isopropyl alcohol; methanol / 1 h / 20 °C

10.1: pyridine / dichloromethane / 1 h / -10 - 0 °C

11.1: sodium iodide / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 - 22 °C

12.1: triethylamine; nickel dichloride; chromium dichloride; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide / tetrahydrofuran / 20.5 h / 22 - 24 °C / Inert atmosphere

12.2: 1 h / 0 - 5 °C

13.1: dmap; pyridine / 3 h / 20 - 23 °C

14.1: zinc; acetic acid / water; tetrahydrofuran / 3 h / 0 - 20 °C

With pyridine; 1H-imidazole; chromium dichloride; hydrogenchloride; dmap; lithium borohydride; water; hydrogen; potassium hexamethylsilazane; acetic acid; triethylamine; sodium iodide; nickel dichloride; zinc; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide; methanesulfonic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 12.1: Nozaki-Hiyama-Kishi Coupling / 14.1: Vasella Fragmentation;

Reference yield:

: 1316278-79-1
C₂₆H₄₇NO₅Si

: 1316279-00-1
C₅₂H₉₀O₁₂SSi₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: zinc / methanesulfonic acid / tetrahydrofuran / 5 h / Reflux

2.1: water; acetic acid / tetrahydrofuran / 10 h / 10 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

4.1: toluene / 0.25 h / 95 °C

5.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 1 h / -30 - -25 °C

6.1: hydrogenchloride / isopropyl alcohol; methanol / 1 h / 20 °C

7.1: pyridine / dichloromethane / 1 h / -10 - 0 °C

8.1: sodium iodide / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 - 22 °C

9.1: triethylamine; nickel dichloride; chromium dichloride; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide / tetrahydrofuran / 20.5 h / 22 - 24 °C / Inert atmosphere

9.2: 1 h / 0 - 5 °C

10.1: dmap; pyridine / 3 h / 20 - 23 °C

11.1: zinc; acetic acid / water; tetrahydrofuran / 3 h / 0 - 20 °C

With pyridine; chromium dichloride; hydrogenchloride; dmap; water; hydrogen; potassium hexamethylsilazane; acetic acid; triethylamine; sodium iodide; nickel dichloride; zinc; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide; methanesulfonic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 9.1: Nozaki-Hiyama-Kishi Coupling / 11.1: Vasella Fragmentation;