rilpivirine tosylate salt

Base Information

Chemical Name:rilpivirine tosylate salt
CAS No.:1399384-91-8
Molecular Formula:C₇H₈O₃S*C₂₂H₁₈N₆
Molecular Weight:538.63
Hs Code.:

Synonyms:rilpivirine tosylate salt

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Chemical Property of rilpivirine tosylate salt

Chemical Property:

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Technology Process of rilpivirine tosylate salt

There total 3 articles about rilpivirine tosylate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 500287-72-9
rilpivirine

: 1399384-91-8
rilpivirine tosylate salt

Guidance literature:: With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 1h;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1399384-91-8
rilpivirine tosylate salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: iodine / 1,4-dioxane; pyridine / 2 h / 0 - 20 °C

2.1: sodium acetate / palladium on activated charcoal / ISOPROPYLAMIDE / 12 h / 140 °C / Inert atmosphere

2.2: 1 h / 60 °C

3.1: toluene-4-sulfonic acid / 1,4-dioxane / 14 h / 100 - 110 °C

4.1: toluene-4-sulfonic acid / acetone / 1 h / 20 °C

With iodine; sodium acetate; toluene-4-sulfonic acid; palladium on activated charcoal; In 1,4-dioxane; pyridine; ISOPROPYLAMIDE; acetone;

Reference yield:

: 4102-53-8
4-iodo-2,6-dimethylaniline

: 1399384-91-8
rilpivirine tosylate salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium acetate / palladium on activated charcoal / ISOPROPYLAMIDE / 12 h / 140 °C / Inert atmosphere

1.2: 1 h / 60 °C

2.1: toluene-4-sulfonic acid / 1,4-dioxane / 14 h / 100 - 110 °C

3.1: toluene-4-sulfonic acid / acetone / 1 h / 20 °C

With sodium acetate; toluene-4-sulfonic acid; palladium on activated charcoal; In 1,4-dioxane; ISOPROPYLAMIDE; acetone;