Technology Process of C28H40N2O3Si
There total 6 articles about C28H40N2O3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H39NO4Si;
With
phthalimide; di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 20 ℃;
for 20h;
Cooling with ice;
With
hydrazine hydrate;
In
ethanol;
at 70 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
1.2: 3 h / 0 - 20 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 18 h
3.1: hydrogen; 10% palladium hydroxide on charcoal / ethanol; acetic acid / 40 h / 38002.6 Torr
4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h
5.1: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
6.1: phthalimide; triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
6.2: 2 h / 70 °C
With
1H-imidazole; lithium borohydride; phthalimide; di-isopropyl azodicarboxylate; 10% palladium hydroxide on charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine;
In
tetrahydrofuran; ethanol; acetic acid; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium borohydride / tetrahydrofuran / 18 h / 20 °C / Cooling with ice
2.1: phthalimide; triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice
2.2: 2 h / 70 °C
With
lithium borohydride; phthalimide; di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
