3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one

Base Information

Chemical Name:3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one
CAS No.:886220-26-4
Molecular Formula:C₁₈H₁₃BrN₂O₃
Molecular Weight:385.217
Hs Code.:

3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3<i>H</i>-[1,3,4]oxadiazol-2-one

Synonyms:3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one

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Chemical Property of 3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one

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Technology Process of 3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one

There total 3 articles about 3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 886220-21-9
C₁₇H₁₀Br₂N₂O₃

: 108-24-7
acetic anhydride

: 886220-26-4
3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one

Guidance literature:: for 0.133333h; microwave irradiation;
DOI:10.1002/jhet.5570430214

Reference yield:

: 84968-90-1
4-bromo-3-[p-(acetyl)phenyl]sydnone

: 886220-26-4
3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaOH / ethanol / 0.13 h / microwave irradiation

2: 86 percent / 0.13 h / microwave irradiation

With sodium hydroxide; In ethanol;
DOI:10.1002/jhet.5570430214

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 886220-26-4
3-{4-[3-(4-bromo-phenyl)-acryloyl]-phenyl}-5-methyl-3H-[1,3,4]oxadiazol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaOH / ethanol / 0.13 h / microwave irradiation

2: 86 percent / 0.13 h / microwave irradiation

With sodium hydroxide; In ethanol;
DOI:10.1002/jhet.5570430214