2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside
CAS No.:1386972-59-3
Molecular Formula:C₆₀H₇₀N₄O₁₁Si
Molecular Weight:1051.32
Hs Code.:

Synonyms:2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside

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Chemical Property of 2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside

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Technology Process of 2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside

There total 1 articles about 2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1386972-58-2
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1386972-59-3
2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1080/07328303.2012.658274

Reference yield:

: trityl chloride polystyrene resin

: 1386972-59-3
2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside

: C₇₉H₈₃N₄O₁₁PolSi

Guidance literature:: trityl chloride polystyrene resin; With pyridine; for 0.0833333h; solid phase reaction;

2'-aminoethyl 4-O-[3-O-acetyl-2-azido-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranosyl]-2,3,6-O-benzyl-β-D-glucopyranoside; With dmap; at 60 ℃; for 48h; solid phase reaction;

In methanol; at 20 ℃; for 1h;
DOI:10.1080/07328303.2012.658274