dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate

Base Information

Chemical Name:dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate
CAS No.:120854-01-5
Molecular Formula:C₂₀H₂₄O₆
Molecular Weight:360.407
Hs Code.:

Synonyms:dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate

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Chemical Property of dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate

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Technology Process of dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate

There total 4 articles about dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 120854-00-4
anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylic acid

: 120854-01-5
dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate

Guidance literature:: In diethyl ether; at 0 ℃;

Reference yield:

: 54585-23-8
(1R,2R,5S,6S)-tricyclo[4.3.1.12,5]undec-3-en-10-one

: 120854-01-5
dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Al-triisopropoxide / acetone; xylene / 12 h / Heating

2: 74 percent / pyridine / 24 h / Ambient temperature

3: 57 percent / tetrabutylammonium bromide, KMnO₄ / H₂O; benzene / 12 h / Ambient temperature

4: 93 percent / diethyl ether / 0 °C

With potassium permanganate; tetrabutylammomium bromide; aluminum isopropoxide; In pyridine; diethyl ether; water; acetone; xylene; benzene;

Reference yield:

: 120925-94-2
anti-tricyclo<4.3.1.1^2,5>undec-3-en-anti-10-ol

: 120854-01-5
dimethyl anti-9-benzoyloxybicyclo<3.3.1>nonane-exo-2,exo-4-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / pyridine / 24 h / Ambient temperature

2: 57 percent / tetrabutylammonium bromide, KMnO₄ / H₂O; benzene / 12 h / Ambient temperature

3: 93 percent / diethyl ether / 0 °C

With potassium permanganate; tetrabutylammomium bromide; In pyridine; diethyl ether; water; benzene;