2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide

Base Information

Chemical Name:2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide
CAS No.:1044870-79-2
Molecular Formula:C₂₀H₂₁N₃O₅
Molecular Weight:383.404
Hs Code.:

Synonyms:2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide

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Chemical Property of 2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide

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Technology Process of 2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide

There total 3 articles about 2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1040044-16-3
2-(4-formyl-2,6-dimethyl-phenoxy)acetamide

: 5004-88-6
4,5-dimethoxyanthranilamide

: 1044870-79-2
2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide

Guidance literature:: With toluene-4-sulfonic acid; sodium hydrogensulfite; In N,N-dimethyl acetamide; at 150 ℃; for 16h;

Reference yield:

: 4959-60-8
4,5-dimethoxy-2-nitrobenzamide

: 1044870-79-2
2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol / 20 h / 2585.81 Torr

2: sodium hydrogensulfite; toluene-4-sulfonic acid / N,N-dimethyl-formamide / 16 h / 150 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid; sodium hydrogensulfite; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 134-96-3
syringic aldehyde

: 1044870-79-2
2-(4-(6,7-dimethoxy-4-oxo-3,4-dihydroquinazolin-2-yl)-2,6-dimethylphenoxy)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Inert atmosphere

1.2: 36 h / 20 °C

2.1: sodium hydrogensulfite; toluene-4-sulfonic acid / N,N-dimethyl-formamide / 16 h / 150 °C / Inert atmosphere

With sodium hydride; toluene-4-sulfonic acid; sodium hydrogensulfite; In N,N-dimethyl-formamide; mineral oil;