trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO₄)

Base Information

• Chemical Name: trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO₄)
• CAS No.: 95099-73-3
• Molecular Formula: C₄₉H₄₃ClN₂O₃P₂PtRh*ClO₄
• Molecular Weight: 1202.73

Synonyms:trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO₄)

Chemical Property of trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO₄)

Chemical Property:

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Technology Process of trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO₄)

There total 4 articles about trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt](ClO4) (95099-71-1) → trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO4) (95099-73-3)

Guidance literature:

With CO; In hexane; toluene; CO bubbled through stirred suspn. of complex in toluene/n-hexane (4/1)for 15 min, kept under CO for 1 h; filtered, washed with toluene/n-hexane; elem. anal.;

Reference yield:

trans-chloro-[1-(p-methoxyphenylimino)-2-(methylimino)propyl]bis(triphenylphosphine)platinum (88887-10-9) → trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO4) (95099-73-3)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; dichloromethane

2: CO / toluene; hexane

With CO; In methanol; hexane; dichloromethane; toluene;

Reference yield:

chloro(C(NC6H4OMe-p)COMe)bis(triphenylphosphine)platinum (78206-31-2,78419-44-0) → trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(carbonyl)2](triphenylphosphine)2Pt](ClO4) (95099-73-3)

Guidance literature:

Multi-step reaction with 3 steps

1: CH₃NH₂ / not given

2: methanol; dichloromethane

3: CO / toluene; hexane

With CH₃NH₂; CO; In methanol; hexane; dichloromethane; toluene;

upstream raw materials:

trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Rh(η4-cyclo-octa-1,5-diene)](triphenylphosphine)2Pt](ClO4)

trans-[chloro-[(1-(p-methoxyphenylimino)-2-(methylimino)propyl)Pd(η3-2-MeC3H4)](triphenylphosphine)2Pt](ClO4)

trans-chloro-[1-(p-methoxyphenylimino)-2-(methylimino)propyl]bis(triphenylphosphine)platinum

chloro(C(NC₆H₄OMe-p)COMe)bis(triphenylphosphine)platinum

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