(+/-)-1-ethyl-2-cyclohexene-1-propanol acetate

Base Information

Chemical Name:(+/-)-1-ethyl-2-cyclohexene-1-propanol acetate
CAS No.:912959-46-7
Molecular Formula:C₁₃H₂₂O₂
Molecular Weight:210.316
Hs Code.:

Synonyms:(+/-)-1-ethyl-2-cyclohexene-1-propanol acetate

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Chemical Property of (+/-)-1-ethyl-2-cyclohexene-1-propanol acetate

Chemical Property:

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Technology Process of (+/-)-1-ethyl-2-cyclohexene-1-propanol acetate

There total 11 articles about (+/-)-1-ethyl-2-cyclohexene-1-propanol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 844655-71-6
(+/-)-1-ethyl-2-cyclohexene-1-propanol

: 912959-46-7
(+/-)-1-ethyl-2-cyclohexene-1-propanol acetate

Guidance literature:: With pyridine; dmap; at 0 - 18 ℃; for 1.5h;
DOI:10.1071/CH05181

Reference yield:

: 17299-34-2
3-ethylcyclohex-2-en-1-one

: 912959-46-7
(+/-)-1-ethyl-2-cyclohexene-1-propanol acetate

Guidance literature:: Multi-step reaction with 9 steps

1.1: NaBH₄ / methanol / 16 h / 0 - 18 °C

2.1: pyridine; DMAP / 10 h / 0 - 18 °C

3.1: lithiium diisopropylamide / tetrahydrofuran; hexane / -78 - 18 °C

3.2: tetrahydrofuran; hexane / 6 h / 66 °C

3.3: 62 percent / tetrahydrofuran; hexane; methanol / 16 h / 18 °C

4.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / 18 °C

5.1: 89 percent / PhI(OAc)2; 4-AcN(H)TEMPO / CH₂Cl₂ / 3 h / 18 °C

6.1: sodium hexamethyldisilazide / tetrahydrofuran; hexane / 0.17 h / 0 °C

6.2: 80 percent / tetrahydrofuran; hexane / 16 h / 0 - 18 °C

7.1: 100 percent / HCl / tetrahydrofuran; H₂O / 16 h / 0 - 18 °C

8.1: 92 percent / NaBH₄ / methanol / 3 h / 0 °C

9.1: 100 percent / DMAP; pyridine / 1.5 h / 0 - 18 °C

With pyridine; hydrogenchloride; dmap; 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; sodium tetrahydroborate; lithium aluminium tetrahydride; [bis(acetoxy)iodo]benzene; sodium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1071/CH05181

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 912959-46-7
(+/-)-1-ethyl-2-cyclohexene-1-propanol acetate

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / 3 h / 0 °C

1.2: 89 percent / HCl / tetrahydrofuran; H₂O / 16 h / 18 °C

2.1: NaBH₄ / methanol / 16 h / 0 - 18 °C

3.1: pyridine; DMAP / 10 h / 0 - 18 °C

4.1: lithiium diisopropylamide / tetrahydrofuran; hexane / -78 - 18 °C

4.2: tetrahydrofuran; hexane / 6 h / 66 °C

4.3: 62 percent / tetrahydrofuran; hexane; methanol / 16 h / 18 °C

5.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / 18 °C

6.1: 89 percent / PhI(OAc)2; 4-AcN(H)TEMPO / CH₂Cl₂ / 3 h / 18 °C

7.1: sodium hexamethyldisilazide / tetrahydrofuran; hexane / 0.17 h / 0 °C

7.2: 80 percent / tetrahydrofuran; hexane / 16 h / 0 - 18 °C

8.1: 100 percent / HCl / tetrahydrofuran; H₂O / 16 h / 0 - 18 °C

9.1: 92 percent / NaBH₄ / methanol / 3 h / 0 °C

10.1: 100 percent / DMAP; pyridine / 1.5 h / 0 - 18 °C

With pyridine; hydrogenchloride; dmap; 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; sodium tetrahydroborate; lithium aluminium tetrahydride; [bis(acetoxy)iodo]benzene; sodium hexamethyldisilazane; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1071/CH05181