Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

Base Information

Chemical Name:Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester
CAS No.:108212-82-4
Molecular Formula:C₃₆H₄₀INO₁₃S₂
Molecular Weight:885.749
Hs Code.:

Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

Synonyms:Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

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Chemical Property of Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

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Technology Process of Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

There total 3 articles about Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₄₇IN₂O₁₅S₄

: 108212-82-4
Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine / CH₂Cl₂; methanol

2: 1.) K₂CO₃ / 1.) MeOH, 5 min

With potassium carbonate; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1021/ja00245a051

Reference yield:

: 108-24-7
acetic anhydride

: C₃₉H₄₇IN₂O₁₅S₂

: 108212-82-4
Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

Guidance literature:: With potassium carbonate; Multistep reaction; 1.) MeOH, 5 min;
DOI:10.1021/ja00245a051

Reference yield:

: 108-24-7
acetic anhydride

: 108232-87-7,138383-03-6
C₃₉H₄₇IN₂O₁₅S₂

: Acetic acid 9-{(2S,3R,4S,5S,6R)-5-[(2S,4S,5S,6R)-5-(4-acetoxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-4-hydroxy-6-methyl-tetrahydro-pyran-2-yloxyamino]-3,4-dihydroxy-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

: 108212-82-4
Acetic acid 9-{(2S,3R,4S,5S,6R)-3,4-dihydroxy-5-[(2S,4S,5S,6R)-4-hydroxy-5-(4-hydroxy-3-iodo-5,6-dimethoxy-2-methyl-benzoylsulfanyl)-6-methyl-tetrahydro-pyran-2-yloxyamino]-6-methyl-tetrahydro-pyran-2-yloxy}-naphtho[2,3-b]thiophen-4-yl ester

Guidance literature:: With potassium carbonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) MeOH, RT, 5 min, 2.) MeOH, 4 deg C, 2 h;
DOI:10.1021/ja00029a030