2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane

Base Information

Chemical Name:2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane
CAS No.:174005-38-0
Molecular Formula:C₁₆H₂₂O₂Si₂
Molecular Weight:302.52
Hs Code.:

Synonyms:2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane

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Chemical Property of 2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane

Chemical Property:

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Technology Process of 2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane

There total 4 articles about 2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 17964-44-2
2,5-dimethyl-2,5-diphenyl-[1,2,5]oxadisilolane

: 174005-38-0
2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 48h; Ambient temperature;
DOI:10.1007/bf01169967

Reference yield:

: 17937-48-3
Si,Si'-dichloro-Si,Si'-dimethyl-Si,Si'-diphenyl-Si,Si'-ethane-1,2-diyl-bis-silane

: 174005-38-0
2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Py, H₂O / dioxane; diethyl ether / 2 h

2: 46 percent / aq. NaOH / dioxane / 48 h / Ambient temperature

With pyridine; sodium hydroxide; water; In 1,4-dioxane; diethyl ether;
DOI:10.1007/bf01169967

Reference yield:

: 1631-82-9
chloro(methyl)phenylsilane

: 174005-38-0
2,5-dihydroxy-2,5-diphenyl-2,5-disilahexane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / H₂PtCl₆ / propan-2-ol / 80 °C

2: 84 percent / Py, H₂O / dioxane; diethyl ether / 2 h

3: 46 percent / aq. NaOH / dioxane / 48 h / Ambient temperature

With pyridine; dihydrogen hexachloroplatinate; sodium hydroxide; water; In 1,4-dioxane; diethyl ether; isopropyl alcohol;
DOI:10.1007/bf01169967