Bis[1,3]dioxolo[4,5]benzo[1,2,3-de:1',2'-g]quinolin-8-one,4-methoxy-

Base Information

Chemical Name:Bis[1,3]dioxolo[4,5]benzo[1,2,3-de:1',2'-g]quinolin-8-one,4-methoxy-
CAS No.:16408-75-6
Molecular Formula:C₁₉H₁₁NO₆
Molecular Weight:349.299
Hs Code.:

Synonyms:8H-Bis[1,3]benzodioxolo[6,5,4-de:5',6'-g]quinolin-8-one,4-methoxy- (9CI); Noraporphin-7-one,4,5,6,6a-tetradehydro-3-methoxy-1,2:9,10-bis(methylenedioxy)- (8CI);Cassamedine

Suppliers and Price of Bis[1,3]dioxolo[4,5]benzo[1,2,3-de:1',2'-g]quinolin-8-one,4-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Bis[1,3]dioxolo[4,5]benzo[1,2,3-de:1',2'-g]quinolin-8-one,4-methoxy-

Chemical Property:

PSA：76.11000
LogP:2.91220

Purity/Quality:: 90.0% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Bis[1,3]dioxolo[4,5]benzo[1,2,3-de:1',2'-g]quinolin-8-one,4-methoxy-

There total 3 articles about Bis[1,3]dioxolo[4,5]benzo[1,2,3-de:1',2'-g]quinolin-8-one,4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49689-91-0
4-methoxy-7-methyl-6,7-dihydro-5H-bis([1,3]dioxolo[4',5':4,5]benzo)[1,2,3-de;1,2-g]quinoline

: 16408-75-6
Cassamedin

Guidance literature:: With peracetic acid; In acetic acid;
DOI:10.1021/jo00918a040

Reference yield:

: 49689-90-9
4-methoxy-5,6-dihydro-bis([1,3]dioxolo[4',5':4,5]benzo)[1,2,3-de;1,2-g]quinoline-7-carboxylic acid ethyl ester

: 16408-75-6
Cassamedin

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄, AlCl₃ / diethyl ether / Heating

2: AcOOH / acetic acid

With peracetic acid; lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; acetic acid;
DOI:10.1021/jo00918a040

Reference yield:

: 49844-61-3
5-(6-bromo-benzo[1,3]dioxol-5-ylmethyl)-9-methoxy-7,8-dihydro-[1,3]dioxolo[4,5-g]isoquinoline; hydrochloride

: 16408-75-6
Cassamedin

Guidance literature:: Multi-step reaction with 3 steps

1: (i) ClCO₂Et, Et₃N, (ii) (irradiation)

2: LiAlH₄, AlCl₃ / diethyl ether / Heating

3: AcOOH / acetic acid

With peracetic acid; lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; acetic acid;
DOI:10.1021/jo00918a040