Technology Process of C39H55NO5Si2
There total 3 articles about C39H55NO5Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methylmagnesium bromide;
In
diethyl ether;
at 0 ℃;
DOI:10.1021/jo301638z
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / acetonitrile / 0 - 20 °C
2: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C
3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C
4: diisobutylaluminium hydride / dichloromethane / -78 °C
5: methylmagnesium bromide / diethyl ether / 0 °C
With
2,6-dimethylpyridine; thionyl chloride; methylmagnesium bromide; diisobutylaluminium hydride; lithium hexamethyldisilazane;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo301638z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C
2: diisobutylaluminium hydride / dichloromethane / -78 °C
3: methylmagnesium bromide / diethyl ether / 0 °C
With
2,6-dimethylpyridine; methylmagnesium bromide; diisobutylaluminium hydride;
In
diethyl ether; dichloromethane;
DOI:10.1021/jo301638z