adamantane-2,6-dione

Base Information

• Chemical Name: adamantane-2,6-dione
• CAS No.: 39751-07-0
• Molecular Formula: C10H12O2
• Molecular Weight: 164.201080
• Mol file: 39751-07-0.mol

Synonyms:2,6-Adamantandione;

Chemical Property of adamantane-2,6-dione

Chemical Property:

• Vapor Pressure: 0.000758mmHg at 25°C
• Melting Point: 323-323.4 °C
• Refractive Index: 1.554
• Boiling Point: 306.7 °C at 760 mmHg
• Flash Point: 114.7 °C
• PSA: 34.14000
• Density: 1.239 g/cm³
• LogP: 1.19060
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

2,6-Adamantanedione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of adamantane-2,6-dione

There total 16 articles about adamantane-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

adamantane-2,6-dione bis-(ethylene)ketal (60797-89-9) → adamantane-2,6-dione (39751-07-0)

Guidance literature:

With hydrogenchloride; for 2h;

DOI:10.1016/0040-4039(94)85347-9

Reference yield: 54.0%

2-Adamantanone (700-58-3) + acetic anhydride (108-24-7) → adamantane-2,6-dione (39751-07-0) + chemantane (20098-14-0) + acetic acid 2-oxo-adamantan-5-yl ester (63382-10-5) + 2,4-adamantanedione (19214-00-7)

Guidance literature:

With pyridine; chromium(VI) oxide; at 20 ℃; for 16h;

DOI:10.1080/00397919908085947

Reference yield: 6.1%

2-Adamantanone (700-58-3) → adamantane-2,6-dione (39751-07-0) + 2,4-adamantanedione (19214-00-7)

Guidance literature:

With oxygen; acetic acid; zinc; 2C5H5N; In pyridine; at 30 ℃; for 12h;

upstream raw materials:

1-Brom-2.6-dioxo-adamantan

2-Adamantanone

adamantane-2,6-dione bis-(ethylene)ketal

diiodomethane

Downstream raw materials:

2,6-dihydroxyadamantane

2,6-dihydroxy-tricyclo<3.3.1.1^3,7>decane