4-methoxybenzyl phosphine

Base Information

• Chemical Name: 4-methoxybenzyl phosphine
• CAS No.: 366491-40-9
• Molecular Formula: C₈H₁₁OP
• Molecular Weight: 154.148

Synonyms:4-methoxybenzyl phosphine

Chemical Property of 4-methoxybenzyl phosphine

Chemical Property:

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Technology Process of 4-methoxybenzyl phosphine

There total 1 articles about 4-methoxybenzyl phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

p-methoxybenzyl chloride (824-94-2) → 4-methoxybenzyl phosphine (366491-40-9) + bis(4-methoxybenzyl)phosphine

Guidance literature:

With phosphan; In potassium hydroxide; dimethyl sulfoxide; at 40 - 45 ℃; for 4h;

DOI:10.1023/A:1012377322193

Reference yield: 82.0%

4-methoxybenzyl phosphine (366491-40-9) → [(4-methoxyphenyl)methyl]phosphinic acid (326480-16-4)

Guidance literature:

With oxygen; In chloroform; at 20 ℃; for 2h;

DOI:10.1023/A:1012377322193

Reference yield:

4-methoxybenzyl phosphine (366491-40-9) → 4-methoxybenzylphosphine oxide

Guidance literature:

With oxygen; In chloroform; at 20 ℃; for 1h;

DOI:10.1023/A:1012377322193

upstream raw materials:

p-methoxybenzyl chloride

Downstream raw materials:

[(4-methoxyphenyl)methyl]phosphinic acid

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