C₂₂H₂₀O₂S

Base Information

Chemical Name:C₂₂H₂₀O₂S
CAS No.:1373403-49-6
Molecular Formula:C₂₂H₂₀O₂S
Molecular Weight:348.466
Hs Code.:

C<sub>22</sub>H<sub>20</sub>O<sub>2</sub>S

Synonyms:C₂₂H₂₀O₂S

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Chemical Property of C₂₂H₂₀O₂S

Chemical Property:

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Technology Process of C₂₂H₂₀O₂S

There total 3 articles about C₂₂H₂₀O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 529-36-2
1-Naphthalenethiol

: C₁₂H₁₄O₃

: 1373403-49-6
C₂₂H₂₀O₂S

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 14h;
DOI:10.1002/anie.201107317

Reference yield:

: 86462-75-1
(E)-5-(tert-butyldimethylsilanyloxy)pent-2-en-1-ol

: 1373403-49-6
C₂₂H₂₀O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

1.2: 0 - 20 °C

2.1: tetrabutyl ammonium fluoride / 1 h / 0 - 20 °C

3.1: sodium periodate; potassium dichromate; nitric acid / water; acetonitrile / 0 - 10 °C

4.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 14 h / 0 - 20 °C

With dmap; sodium periodate; potassium dichromate; tetrabutyl ammonium fluoride; nitric acid; sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201107317

Reference yield:

: 171857-02-6
trans-1-(benzyloxy)-5-(t-butyldimethylsilyloxy)-2-pentene

: 1373403-49-6
C₂₂H₂₀O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / 1 h / 0 - 20 °C

2: sodium periodate; potassium dichromate; nitric acid / water; acetonitrile / 0 - 10 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 14 h / 0 - 20 °C

With dmap; sodium periodate; potassium dichromate; tetrabutyl ammonium fluoride; nitric acid; dicyclohexyl-carbodiimide; In dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201107317