(S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate

Base Information

Chemical Name:(S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate
CAS No.:1446512-85-1
Molecular Formula:C₂HF₃O₂*C₁₂H₁₂N₄O₅
Molecular Weight:406.275
Hs Code.:

Synonyms:(S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate

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Chemical Property of (S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate

Chemical Property:

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Technology Process of (S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate

There total 5 articles about (S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1446513-04-7
(S)-N-((3-(tert-butoxy)-2-((tert-butoxycarbonyl)amino)-3-oxopropoxy)carbonyl)-3-phenylsydnonimine

: 76-05-1
trifluoroacetic acid

: 1446512-85-1
(S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate

Guidance literature:: In dichloromethane; at 0 ℃; for 18h;
DOI:10.1039/c3ob41047a

Reference yield:

: 62-53-3
aniline

: 1446512-85-1
(S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; sodium iodide / acetone / 12 h / 20 °C / Darkness

2.1: isopentyl nitrite / diethyl ether / 16 h / 20 °C / Darkness

2.2: 0.25 h / 20 °C

3.1: triethylamine / dichloromethane / 16 h / -20 - 20 °C

4.1: acetonitrile / 18 h / Reflux

5.1: dichloromethane / 18 h / 0 °C

With potassium carbonate; triethylamine; sodium iodide; isopentyl nitrite; In diethyl ether; dichloromethane; acetone; acetonitrile;
DOI:10.1039/c3ob41047a

Reference yield:

: 3009-97-0
N-phenylglycinonitrile

: 1446512-85-1
(S)-N-((2-amino-2-carboxyethoxy)carbonyl)-3-phenylsydnonimine trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: isopentyl nitrite / diethyl ether / 16 h / 20 °C / Darkness

1.2: 0.25 h / 20 °C

2.1: triethylamine / dichloromethane / 16 h / -20 - 20 °C

3.1: acetonitrile / 18 h / Reflux

4.1: dichloromethane / 18 h / 0 °C

With triethylamine; isopentyl nitrite; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1039/c3ob41047a