tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate

Base Information

Chemical Name:tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate
CAS No.:220821-65-8
Molecular Formula:BF₄*C₂₆H₃₆MoO₃P
Molecular Weight:610.288
Hs Code.:

Synonyms:tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate

Suppliers and Price of tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate

There total 1 articles about tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 12176-06-6
hydrido(tricarbonyl)(cyclopentadienyl)molybdenum

: 83115-12-2
(2,4,6-tri-tert-butylphenyl)phosphine

: 341-02-6
trityl tetrafluoroborate

: 220821-65-8
tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate

Guidance literature:: In dichloromethane; N2-atmosphere; mixing equimolar amts. of (Cp(CO)3Mo)BF4 (prepd. from Cp(CO)3MoH and trityl tetrafluoroborate) with phosphine at -78°C indark, warming to room temp., stirring for 2 h; concn. (vac.), pptn. on addn. of ether and pentane, drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(98)00947-4

Reference yield: 89.0%

: 220821-65-8
tricarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenylphosphane]molybdenum(II) tetrafluoroborate

: 220821-67-0
tricarbonyl(η(5)-cyclopentadienyl)molybdenum(II)[2,4,6-tri(tert-butyl)-phenyl]phosphane

Guidance literature:: With Et₃N; In methyl cyclohexane; byproducts: (Et3NH)BF4; N2-atmosphere; mixing equimolar amts. of Mo-complex with Et3N at 0°C, stirring (room temp., 1 h); filtration off of (Et3NH)BF4, solvent removal (vac.), washing (pentane), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(98)00947-4