N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal

Base Information

Chemical Name:N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal
CAS No.:944282-27-3
Molecular Formula:C₂₇H₃₃N₃O₄
Molecular Weight:463.577
Hs Code.:

Synonyms:N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal

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Chemical Property of N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal

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Technology Process of N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal

There total 11 articles about N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 944282-26-2
N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinol

: 944282-27-3
N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal

Guidance literature:: N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinol; With Dess-Martin periodane; In dichloromethane; at 0 ℃; for 1h;

With sodium hydrogencarbonate; sodium thiosulfate; In dichloromethane; water; ethyl acetate; at 0 ℃;

Reference yield:

: 944282-12-6
1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexanecarboxylic acid phenylmethyl ester

: 944282-27-3
N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; water / tetrahydrofuran / Heating / reflux

1.3: 1 h

2.1: N,N-dimethyl-formamide

3.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

3.2: 0 °C

With sodium hydroxide; water; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 944282-07-9
1-[[[4-(chloromethyl)phenyl]carbonyl]amino]cyclohexanecarboxylic acid methyl ester

: 944282-27-3
N-[[1-[[[4-(4-morpholinylmethyl)phenyl]carbonyl]amino]cyclohexyl]carbonyl]-L-phenylglycinal

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1 h / Heating / reflux

2.1: sodium hydroxide; water / tetrahydrofuran / Heating / reflux

2.3: 1 h

3.1: N,N-dimethyl-formamide

4.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

4.2: 0 °C

With sodium hydroxide; water; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;