Technology Process of C44H58O8
There total 2 articles about C44H58O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H18O5;
With
2,4,6-trichlorobenzoyl chloride; triethylamine;
In
toluene;
at 20 ℃;
for 3h;
C31H42O4;
With
dmap;
In
toluene;
at 50 ℃;
for 1.5h;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C
2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C
2.2: 1.5 h / 50 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; triethylamine;
In
tetrahydrofuran; water; toluene; tert-butyl alcohol;
2.1: |Yamaguchi Lactonization / 2.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; water;
at 20 ℃;
for 1h;
DOI:10.1016/j.tet.2013.02.008