Technology Process of C29H31NO8S
There total 5 articles about C29H31NO8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
toluene;
at 20 ℃;
Inert atmosphere;
DOI:10.1016/j.tet.2011.09.011
- Guidance literature:
-
Multi-step reaction with 2 steps
1: samarium diiodide / tetrahydrofuran; methanol / 0 °C / Inert atmosphere
2: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 20 °C / Inert atmosphere
With
samarium diiodide; di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran; methanol; toluene;
2: Mitsunobu reaction;
DOI:10.1016/j.tet.2011.09.011
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ethylmagnesium bromide; lithium chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere
1.2: 12 h / 20 °C / Inert atmosphere
2.1: water; calcium carbonate; methyl iodide / acetonitrile / 40 °C / Inert atmosphere
3.1: samarium diiodide / tetrahydrofuran; methanol / 0 °C / Inert atmosphere
4.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 20 °C / Inert atmosphere
With
samarium diiodide; di-isopropyl azodicarboxylate; ethylmagnesium bromide; water; triphenylphosphine; calcium carbonate; lithium chloride; methyl iodide;
In
tetrahydrofuran; methanol; diethyl ether; toluene; acetonitrile;
4.1: Mitsunobu reaction;
DOI:10.1016/j.tet.2011.09.011
