C₁₄H₂₄BNO

Base Information

• Chemical Name: C₁₄H₂₄BNO
• CAS No.: 949096-25-7
• Molecular Formula: C₁₄H₂₄BNO
• Molecular Weight: 233.162
• Mol file: 949096-25-7.mol

Synonyms:C₁₄H₂₄BNO

Chemical Property of C₁₄H₂₄BNO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₄H₂₄BNO

There total 1 articles about C₁₄H₂₄BNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lithium triethylborohydride (22560-16-3) + 4-methoxybenzonitrile (874-90-8) → C14H24BNO (949096-25-7)

Guidance literature:

lithium triethylborohydride; 4-methoxybenzonitrile; In tetrahydrofuran; at 0 ℃; for 2h;

With methanol; In tetrahydrofuran; at 0 ℃; for 0.5h;

DOI:10.3987/COM-10-S(E)95

Reference yield:

C14H24BNO (949096-25-7) + (+)-B-allyldiisopinocampheylborane → (1S)-1-(4-methoxyphenyl)but-3-en-1-amine (188425-29-8)

Guidance literature:

C₁₄H₂₄BNO; (+)-B-allyldiisopinocampheylborane; With methanol; In tetrahydrofuran; at -78 ℃;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 25 ℃; for 12h; enantioselective reaction; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.06.076

Reference yield:

1-methoxy-2-methyl-1-trimethylsiloxy-1-propene (31469-15-5) + C14H24BNO (949096-25-7) → methyl 3-amino-2,2-dimethyl-3-(4-methoxyphenyl)propanoate

Guidance literature:

C₁₄H₂₄BNO; With zinc(II) iodide; In diethyl ether; at 20 ℃; for 0.5h;

1-methoxy-2-methyl-1-trimethylsiloxy-1-propene; In diethyl ether; at 20 ℃; for 2h;

DOI:10.3987/COM-10-S(E)95

upstream raw materials:

lithium triethylborohydride

4-methoxybenzonitrile

Downstream raw materials:

3,3-dimethyl-4-(4-methoxyphenyl)-azetidin-2-one

(1S)-1-(4-methoxyphenyl)but-3-en-1-amine

(S)-N-(t-butoxycarbonyl)-1-(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-1-amine