3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride

Base Information

• Chemical Name: 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride
• CAS No.: 108306-65-6
• Molecular Formula: C₁₁H₉N₃OS₂*ClH
• Molecular Weight: 299.805
• Mol file: 108306-65-6.mol

Synonyms:3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride

Chemical Property of 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride

There total 2 articles about 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1-(N-Benzoylthiocarbamoyl)-2-imidazolidinethione (108324-95-4) → 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride (108306-65-6)

Guidance literature:

With hydrogenchloride; dihydrogen peroxide; In ethanol; for 0.0833333h; Heating;

DOI:10.1055/s-1986-33422

Reference yield:

Benzoyl isothiocyanate (532-55-8) → 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride (108306-65-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 56 percent / acetone / 4 h / Heating

2: 84 percent / conc. HCl, 30percent H₂O₂ / ethanol / 0.08 h / Heating

With hydrogenchloride; dihydrogen peroxide; In ethanol; acetone;

DOI:10.1055/s-1986-33422

Reference yield: 80.0%

3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride (108306-65-6) → 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> (108306-66-7)

Guidance literature:

With ammonium hydroxide; In ethanol; at 20 ℃;

DOI:10.1055/s-1986-33422

upstream raw materials:

1-(N-Benzoylthiocarbamoyl)-2-imidazolidinethione

Benzoyl isothiocyanate

Downstream raw materials:

3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole>

1-benzoyl-3-phenylthiourea

O-Propyl-N-benzoylcarbamate

5-Phenyl-3-(2-thioxo-1-imidazolidinyl)-2H-1,2,4-triazole