C₃₀H₄₄N₆

Base Information

• Chemical Name: C₃₀H₄₄N₆
• CAS No.: 883107-23-1
• Molecular Formula: C₃₀H₄₄N₆
• Molecular Weight: 488.72
• Mol file: 883107-23-1.mol

Synonyms:C₃₀H₄₄N₆

Chemical Property of C₃₀H₄₄N₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₀H₄₄N₆

There total 1 articles about C₃₀H₄₄N₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C16H23N3 + N,N-diethyl-N'-(4-tert-butyl-2-iodophenyl)triazene (191231-71-7) → C30H44N6 (883107-23-1)

Guidance literature:

With triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 55 ℃;

DOI:10.1246/cl.2006.168

Reference yield: 90.0%

C30H44N6 (883107-23-1) → C22H24I2 (883107-20-8)

Guidance literature:

With methyl iodide; at 125 ℃; sealed tube;

DOI:10.1246/cl.2006.168

Reference yield:

C30H44N6 (883107-23-1) → C51H50O

Guidance literature:

Multi-step reaction with 4 steps

1: 90 percent / MeI / 125 °C / sealed tube

2: 52 percent / CH₃(C₈H₁₇)3NCl; PPh₃; KOH / Pd(PPh₃)4; CuI / benzene; H₂O / 85 °C

3: 92 percent / K₂CO₃ / Pd(PPh₃)4 / tetrahydrofuran / Heating

4: 92 percent / aq. TFA / CH₂Cl₂ / 20 °C

With potassium hydroxide; potassium carbonate; triphenylphosphine; trifluoroacetic acid; methyl iodide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; water; benzene; 2: double Sonogashira coupling / 3: Suzuki-Miyaura coupling;

DOI:10.1246/cl.2006.168

upstream raw materials:

N,N-diethyl-N'-(4-tert-butyl-2-iodophenyl)triazene

Downstream raw materials:

C₂₂H₂₄I₂

C₅₃H₅₆O₂