Technology Process of C34H48O3Si2
There total 8 articles about C34H48O3Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); caesium carbonate;
In
N,N-dimethyl-formamide;
at 50 ℃;
DOI:10.1016/j.tetlet.2007.01.024
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 97 percent / imidazole; DMAP / dimethylformamide / 60 °C
2.1: O3 / methanol / -78 °C
2.2: NaBH4 / methanol / 0 °C
3.1: imidazole; DMAP / CH2Cl2; dimethylformamide / 20 °C
4.1: aq. TsOH / acetone / 50 °C
5.1: hydrazine; TEA / ethanol / 100 °C
5.2: 93 percent / I2; DBU / diethyl ether / 0 - 20 °C
6.1: 100 percent / Cs2CO3; Pd(PPh3)4 / dimethylformamide / 50 °C
With
1H-imidazole; dmap; tetrakis(triphenylphosphine) palladium(0); TEA; caesium carbonate; toluene-4-sulfonic acid; ozone; hydrazine;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
6.1: Suzuki-Miyaura coupling reaction;
DOI:10.1016/j.tetlet.2007.01.024
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrazine; TEA / ethanol / 100 °C
1.2: 93 percent / I2; DBU / diethyl ether / 0 - 20 °C
2.1: 100 percent / Cs2CO3; Pd(PPh3)4 / dimethylformamide / 50 °C
With
tetrakis(triphenylphosphine) palladium(0); TEA; caesium carbonate; hydrazine;
In
ethanol; N,N-dimethyl-formamide;
2.1: Suzuki-Miyaura coupling reaction;
DOI:10.1016/j.tetlet.2007.01.024