C₂₇H₂₉N₃O₆

Base Information Edit

Chemical Name:C₂₇H₂₉N₃O₆
CAS No.:1401413-68-0
Molecular Formula:C₂₇H₂₉N₃O₆
Molecular Weight:491.544
Hs Code.:
Mol file:1401413-68-0.mol

C<sub>27</sub>H<sub>29</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₂₇H₂₉N₃O₆

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Chemical Property of C₂₇H₂₉N₃O₆ Edit

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Technology Process of C₂₇H₂₉N₃O₆

There total 9 articles about C₂₇H₂₉N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₂₇H₂₇N₃O₆

: 1401413-68-0
C₂₇H₂₉N₃O₆

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; In dichloromethane; at -78 ℃; for 1h;

Reference yield:

: 14131-63-6
D-glucosamine hydrochloride

: 1401413-68-0
C₂₇H₂₉N₃O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydrogencarbonate / water / 0.5 h / 20 °C

1.2: 4.5 h / 20 °C

2.1: pyridine / 0 - 20 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C

4.1: zinc; acetic acid / dichloromethane; methanol / 1 h / 0 - 20 °C / Inert atmosphere

5.1: sodium methylate / dichloromethane; methanol / 2 h / 20 °C

5.2: pH ~ 7

6.1: potassium carbonate; triflic azide / zinc(II) chloride / dichloromethane; water; methanol / 20 °C

7.1: camphorsulfonic acid / toluene / 2 h / 20 °C

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

9.1: trifluorormethanesulfonic acid; triethylsilane / dichloromethane / 1 h / -78 °C

With pyridine; triethylsilane; trifluorormethanesulfonic acid; triflic azide; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; zinc; zinc(II) chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 122210-05-3
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranose

: 1401413-68-0
C₂₇H₂₉N₃O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C

2.1: zinc; acetic acid / dichloromethane; methanol / 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium methylate / dichloromethane; methanol / 2 h / 20 °C

3.2: pH ~ 7

4.1: potassium carbonate; triflic azide / zinc(II) chloride / dichloromethane; water; methanol / 20 °C

5.1: camphorsulfonic acid / toluene / 2 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

7.1: trifluorormethanesulfonic acid; triethylsilane / dichloromethane / 1 h / -78 °C

With triethylsilane; trifluorormethanesulfonic acid; triflic azide; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; potassium carbonate; acetic acid; zinc; zinc(II) chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;